Fluorosugars: synthesis of the 2,3,4-trideoxy-2,3,4-trifluoro hexose analogues of D-glucose and D-altrose and assessment of their erythrocyte transmembrane transport.

نویسندگان

  • Stefano Bresciani
  • Tomas Lebl
  • Alexandra M Z Slawin
  • David O'Hagan
چکیده

The 2,3,4-trideoxy-2,3,4-trifluoro hexose analogues of d-glucose and d-altrose were prepared and characterised and these novel sugar analogues were explored by 2D-(19)F-EXSY NMR for their potential to cross erythrocyte (red blood cell) membranes, by comparison with the well known capacity of erythrocytes to transport d-glucose.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Structure of the O-specific polysaccharide from the lipopolysaccharide of Psychrobacter cryohalolentis K5(T) containing a 2,3,4-triacetamido-2,3,4-trideoxy-L-arabinose moiety.

A novel constituent of bacterial polysaccharides, 2,3,4-triacetamido-2,3,4-trideoxy-L-arabinose, was found in the O-specific polysaccharide from the lipopolysaccharide of Psychrobacter cryohalolentis K5(T) and identified by 1D and 2D (1)H and (13)C NMR studies of the polysaccharide and a disaccharide obtained by solvolysis of the polysaccharide with triflic acid. The following structure of the ...

متن کامل

Application of dimeric and monomeric ortho-palladated complexes as an efficient catalysts for Heck cross-coupling reaction

The catalytic acvtivity of dimeric and monomeric ortho-palladated complexes [Pd{C6H2(CH2NH2-(OMe)2,3,4}(µ-Cl)]2)2) and [Pd{C6H2(CH2NH2-(OMe)2,3,4}Cl(PPh3)](3), was investigated in Heck cross-coupling reaction. These complexes are more active and efficient catalysts for Heck cross-coupling reaction. The palladium complexes 2 and 3 is employed in the Heck cross-coupling reaction between styrene a...

متن کامل

اثر سایپروهپتادین (CYP) بر میزان گلوکز خون و گلیکوژن کبدی در موش های صحرایی (رت)

Background and Purpose: Çyproheptadine (ÇYP) is an antihistaminic and antiserotonine agent with specific property which differentiates it from the other antihistaminics and antiserotonic agent. The appetite stimulating effect of (ÇYP) is well documented in man but its effects on the blood glucose and liver glycogen are not the same. Hence this study was conducted to determine the effects o...

متن کامل

SYNTHESIS AND SPECTROSCOPIC STUDIES OF THIOCYANATO -DERIVATIVES OF CU-Mo-S CLUSTERS

The complexes [MoS (CUNCS) ] w hen x = 2,3,4 and [MoOS , (CUNCS) ] when y = 2, 3 have been prepared by the reaction of CuSCN with [P(C H ) ] [MoS ] or [P(C H ) ] [MOOS ] in dry degassed acetone or DMFsolution and recrystallized from dichloromethane, the attempted preparation of [MoS (AgSCN) ] and [MOOS (AgSCN) ] failed. The Raman, IR, UV/VIS, C-nmr and Mo-nmr spectra of the co...

متن کامل

Entrapment–D-(+)-Glucose Water Nanodroplet: Synthesis and Dynamic Light Scattering

In the present research, the D-(+)-Glucose–confined water nanodroplets with mean size in the range of 6-11 nm were synthesized at D-(+)-Glucose different concentrations by AOT reverse micelles (RMs) method as a function of mass fraction of droplet (MFD) at the constant water-to-surfactant molar ratio ( W=40). The dynamic light scattering of the nano-sized water droplets containing the D-(+)-Glu...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Chemical communications

دوره 46 30  شماره 

صفحات  -

تاریخ انتشار 2010